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Hermann GN, Becker P, Bolm C (2015) Mechanochemical rhodium (III)-catalyzed C-H bond functionalization of acetanilides under solventless conditions in a ball mill. Angew Chem Int Ed Engl 54:7414–7417. doi: 10.1002/anie.201502536
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Boldyrev et al. (), used a planetary ball mill to prepare amorphous co-ground mixture of sulfathiazole with polyvinylpyrrolidone. Amorphization of indomethacin was achieved by milling it with silica or polyvinylpyrrolidone ( 6 ).
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A series of liquid crystal molecules with two Schiff base linking units and a cinnamaldehyde core with different terminal groups were synthesized and characterized. The intermediates of 4-heptyloxybenzaldehyde (1a) and 4-dodeyloxybenzaldehyde (1b) were synthesized through the alkylation of 4-hydroxybenzaldehyde with a series of bromoalkane. A condensation reaction of cinnamaldehyde, …
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Parastagonospora nodorum is a pathogen of wheat that affects yields globally. Previous transcriptional analysis identified a partially reducing polyketide synthase (PR-PKS) gene, SNOG_00477 ( SN477 ), in P. nodorum that is highly upregulated during infection of wheat leaves. Disruption of the corresponding SN477 gene resulted in the loss of production of two compounds, which we identified as ...
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Solvent-free micromechanical oxidation of graphite flakes in presence of oxidants KMnO 4 or (NH 4)2S 2 O 8, was used a planetary ball mill for the synthesis of GO (Posudievsky et al., 2012). Depending upon the use of an oxidizing agent and the external energy used, the …
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Mechanochemical Rhodium(III)-Catalyzed C H Bond Functionalization of Acetanilides under Solventless Conditions in a Ball Mill. Angewandte Chemie 2015, 127 (25) , 7522-7525. DOI: 10.1002/ange.201502536. Gary N
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· Shells were finely crushed into powder in a ball mill for 2 h. 2.2. Electroless nickel-phosphorus coating on CSP (NiP/CSP) The electroless bath composition and operating parameters are shown in …
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